Solid-phase microextraction method for headspace analysis of volatile compounds in bread crumb

From: Cereal Chemistry | Date: May 1, 2003| Author: | Copyright information

ABSTRACT

A solid-phase microextraction method was developed to analyze volatile compounds in bread crumb. Three different fibers usually used to determine volatile compounds in foodstuffs were tested, and Carboxen/ Polydimethylsiloxane showed the best extraction efficiency. This method can determine "65 compounds, although only the main compounds responsible for the crumb aroma profile (6 alcohols, 5 aldehydes, 5 acids, and 2 ketones) were evaluated quantitatively with a relative standard deviation <20% and limits of detection were 1-18 mg/kg. All the compounds showed a good linearity in ...

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